By Parry R.W. (ed.)
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Extra info for Inorganic syntheses
It is insoluble in water and nonpolar organic solvents but soluble in polar organic solvents such as CsHsN02 and H2CCl2. The cation can be precipitated as the reheckate* and hexafluorophosphate from aqueous solution; however, the latter is quite soluble in water. B. CYCLOHEXENE(CYCL0PENTADIENYL)IRON DICARBONYL HEXAFLUOROPHOSPHATE-PREPARATIONS MADE WITH THE AID OF LEWIS ACIDS (D i o a r b o n y I ( a y o 1 o h s e ) a y ~ o ~ n ~ ~ e Hexafiuorophoephate ny~n 1 Olefins do not react with cyclopentadienyliron dicarbonyl halides by themselves.
Am. Chem. , 89,3071 (1967). 7 . A. Misono, Y. Uchida, M. K s e , Chem. , 981 (1968). 4. TRIHYDRIDO-TRIS(TRIPHENYLPH0SPHINE)COBALTOII) AND HYDRIDO(NITROGEN)-TRIS- (TRIPHENYLPHOSPHINE)COBALT(I) Submitted by A. SACCO* and M. ROSSI* Chsolred by FRANK BOTTOMLEYt and A. D. ALLENt Molecular nitrogen complexes of cobalt have been reported by three research groups. 1-4 Preparation of the compound-now * Istituto di Chimica Generale e Inorganica, Universita di Bari, Italy. t Lash-Miller Chemical Laboratories, University of Toronto,Toronto 5, Ontario, Canads.
C. te] ~~eny~n) If cyclopentadienyliron dicarbonyl halides are allowed to react with themselves in the presence of Lewis acids, cations are formed in which the new substituent is the cyclopentadienyliron dicarbonyl halide itself, for example, [CsHsFe(CO)2-X-(CO)r FeCaHa]+(X = C1, Br, I). l~ In the latter two cases the hexafluorophosphate salts can be obtained. , aniline, pyridine, benzonitde, acetonitrile, acrylonitrile, with the formation of the corresponding [CaHaFe(CO)2L]+ cations and the parent halide.